Anyone notice diacetyl from Big dry hopping?

Discussion in 'Homebrewing' started by Brew_Betty, Nov 23, 2018.

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  1. Brew_Betty

    Brew_Betty Initiate (0) Jan 5, 2015 Wisconsin

    I can't be totally sure Expectation Bias is something you can reliably resist right now. However, it appears you are moving in the proper direction of trusting your palate regardless of what science or even popular opinion says about brewing proper beer. Do whatever you have to do to make beer that tastes great to you. Try to forget about how you made the beer you are tasting before passing judgement.

    What do you think is hypothetically wrong with leaving dry hops in the keg? They surrender their goods in 2 days or less. If they are bad to leave in the keg, they must be releasing something that takes longer than a week to extract. What do you suppose that is?
     
  2. billandsuz

    billandsuz Pooh-Bah (2,097) Sep 1, 2004 New York
    Pooh-Bah

    Over 14 years at this site and I thought I had seen it all. And trust me, I've seen a lot. Never bothered to ignore a member until just now.
    That has got to make you proud.
     
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  3. invertalon

    invertalon Pooh-Bah (2,249) Jan 27, 2009 Ohio
    Pooh-Bah Trader

    @Brew_Betty

    I have read in the past a few articles/write ups that mention the increase in grassy/earthy notes if in contact with the beer too long. Perhaps that is the character that I pickup as muddled? So while you are trapping all the oils/aroma in the keg, over a few weeks when the green matter breaks down or whatever, perhaps that is what I pickup as the fall off of my IPA. Not so much that the aroma is gone, just changed (for the worse). It doesn't sound too far off.

    @thebriansmaude sent me this article: http://scottjanish.com/examination-...s-for-achieving-maximum-hop-aroma-and-flavor/

    Which also had an interesting tidbit, relative to oil levels in the samples of hopped beer (done in a keg):

    "Here we can see their results, which show the concentration of linalool tested at 3 different stages of the dry hop (day 1, day 4, and day 7). Interestingly, the oils were almost completely extracted on the first full day of dry hopping and even decreased after day 4! Nearly identical results were found when the myrcene concentration levels were tested (second graph), with myrcene dropping after day 1".

    I tried to look for more data, but in my short look don't see too much on what contact times do in various situations (fermentation dry hop, keg hop, spunded kegs, etc...). But maybe this is a clue to why keg hopping may, or may not be, ideal... Especially relative to how quickly it takes to drink that entire keg. In my case, my beers are usually on for an average of 2-3 months... While other people I'm sure go through their kegs in just 3-4 weeks.

    And I recall back with my old techniques, not noticing the same type of drop off as I do with the newer methods detailed in my previous post.
     
  4. Brew_Betty

    Brew_Betty Initiate (0) Jan 5, 2015 Wisconsin

    That is a very complicated good question. The answer depends on what your intentions are for the acid addition to keg hopped beer and the buffering capacity of the beer in the keg. So I can't reliably give you a number that will automatically please you.

    I acidify a hoppy keg for flavor enhancement, not diacetyl reduction or refermentation mitigation. My mash water and sparge water target 5.2, but they aren't checked with a meter anymore. I used my pH meter frequently at various stages of brewing for several years. Took copious notes. The meter broke. Then I brewed beer while using the pH force.

    When I had a pH meter, my IPAs were in the 4.2-4.7 range before kegging. The keg citric acid addition was intended to be a flavor enhancer and pH was never measured.

    I use 0.5tsp-1.25tsp of citric acid in the keg as a citrus/fruit hop flavor enhancer depending on the recipe. However, the buffering capacity of your beer may require a different range. Plus, different acids give different flavor results with the same acidity. The purpose of using citric acid is to complete the flavor of citrus fruits. The hops provide citrus flavor, the malt provides mild sugar, the citric acid connects the dots.

    Other acids provide similar acidity at the same dose, but have a different impact on flavor perception. Phosphoric has neutral flavor, but it requires a much higher dose to match the acidity of lactic, citric or tartaric acid. Lactic acid makes beer taste and smell sour above a certain threshold. Citric acid makes an IPA taste like Gatorade above a certain threshold. Tartaric acid should be used conservatively with caution. It's what makes sour patch kids sour. It can not be used at the same rate as lactic or citric acid, but it produces similar acidity.

    So the answer to your question is highly dependant on these variables and what you want to achieve. You already had at least one successful keg hop acidification, so you can use this information and build from there.
     
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  5. Brew_Betty

    Brew_Betty Initiate (0) Jan 5, 2015 Wisconsin

    Oh no, Billy. Say it isn't so! You're dramatically announcing Ignore after several years of Brew Betty silence and two current forthright comments that you can't refute?

    Three BAs made the same claim a few years ago. At least one doesn't Ignore me right now. Quite frankly, your public proclamation of Ignore is the most unjustified and I'm totally fine if you never talk to me again. No hard feelings at all. If my legit words irritate you and you can't refute them, then Ignore is a very safe space for you.

    Before you really ignore me, can you please give us some advice regarding the use of gelatin for old time's sake?
     
  6. Brew_Betty

    Brew_Betty Initiate (0) Jan 5, 2015 Wisconsin

    Hop oils extract quickly when they aren't bound by bags. It takes 1-2 days. I already said that and you agree. However, it takes longer to extract hop oils if they are in hop bags and bags are less efficient. A blogger people mention said so because Hopsteiner says so.

    You can't find any information regarding hops kept cold in the keg for months? That is because you are ignoring the opinions of thousands of homebrewers that keep the hops in the keg with very good results. Many of them win awards consistently. Pros don't need to leave hops in the keg or bottle. There is no reason to study it professionally.

    So, I'll ask it again with different words. What do you think hops in the keg are doing to wreck our beers?

    "The proof is in the pudding", said the pudding samplers to the advanced food scientists employed by a very large company that has made billions selling pudding. The samplers' taste was not aligned with the scientist's Expectation Bias. The pudding was an economic home run, though.
     
  7. invertalon

    invertalon Pooh-Bah (2,249) Jan 27, 2009 Ohio
    Pooh-Bah Trader

    Also, thousands of breweries have just as good, or better results without having hops in kegs/bottles/cans (usually...). So I'd say it's not exactly a requirement of making bright, aromatic beer. Its been done without for a long time now.

    I never said hops are wrecking anyone beers. I said for MY beers, I dont like the end result and had better IPA before keg hopping.

    Either way works of the brewer/drinker is happy. Just sharing my own experience, in which my own process is always evolving. Keg hopping just didnt do it for me, yet at least!
     
  8. EvenMoreJesus

    EvenMoreJesus Initiate (0) Jun 8, 2017 Pennsylvania

    I think these are the important bits as to why you didn't get any hop creep or VDKs. Between cold crashing to 60F, dry hopping starting at 60F, cold crashing to serving temperature, and using 1098 ( http://www.wyeastlab.com/yeast-strain/british-ale ), I think that the opportunities for your yeast to ferment any sugars broken down by any hop derived enzymes are pretty low.
     
  9. Brew_Betty

    Brew_Betty Initiate (0) Jan 5, 2015 Wisconsin

    I really appreciate your effort here, but 1098 reliably ferments beer at lower temperatures than Wyeast specifies. It can demolish most of a 1.070 wort held at 60-602F for 4 days. The next step is to finish it with some heat at 70-75F, then soft crash it back down to 60F. A really Cold crash is NOT required in this context. Let it rest for a few days at 60F. Clear, kegable beer happens at day 10-11. The same conditions provide enough yeast to bottle carbonate a full batch within 2 weeks. Therefore, your assertion that 1098 is not capable of fermenting at this stage is bogus.
     
  10. EvenMoreJesus

    EvenMoreJesus Initiate (0) Jun 8, 2017 Pennsylvania

    Fair enough. I don't use that yeast strain, so I really wouldn't know. What I do know, anecdotally, is that I use a Citra a LOT and I've never had any beer overcarbonate after dry hopping or produce VDKs. No actual science in that observation, but it IS one data point.
     
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  11. wasatchback

    wasatchback Pooh-Bah (1,574) Jan 12, 2014 Tajikistan
    Pooh-Bah Trader

    I believe in the mbaa podcast the guys talking about how the Citra they studied rarely caused any refermentation.
     
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  12. dmtaylor

    dmtaylor Savant (1,149) Dec 30, 2003 Wisconsin

    I think you're right. They found that each hop behaved a little different and Citra was one that didn't seem to have any effect at all. Palisade hop definitely had a huge impact on my beer. I doubt anyone knows the exact effects of most other hop varieties quite yet. Will take another decade or two to gather all that data and for people to agree that it actually matters (which it does).
     
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  13. chavinparty

    chavinparty Zealot (653) Jan 4, 2015 New Hampshire

    Citra for the win. @Brew_Betty maybe it’s your appetite for Citra that has kept you from the creep experience you’re looking for.
     
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  14. VikeMan

    VikeMan Grand Pooh-Bah (3,067) Jul 12, 2009 Pennsylvania
    Pooh-Bah

    I assume you mean me. I un-ignore after about 6-12 months or so. Only one (he whose name must not be spoken) has ever gone back on the naughty list after coming off.

    FWIW, I'm enjoying your recent contributions and signal to noise ratio.
     
  15. TheHumanTorch

    TheHumanTorch Devotee (353) Jul 19, 2013 Connecticut

    At the craft brewers conference this year there was a seminar on diacetyl after dry hopping. My memory of it: Allagash was noticing carbonation levels higher than expected in their hoppy table beer. They found that the beer was refermenting in the bottle. The cause was a small dose of alpha and beta amylase present in the dry hop. These enzymes causing a slow transformation of complex sugars into simple. The fermentation was tracked out over months and the fermentation never stalled.

    Diacetyl comes into play because often times beers dry hopped post fermentation do not have an opportunity to clean up the refermentation byproducts.
     
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  16. GreenKrusty101

    GreenKrusty101 Initiate (0) Dec 4, 2008 Nevada

    Seems like a non-problem since the overwhelming majority of dry hopped beers are consumed relatively fresh. What time-frames were they talking?
     
  17. GreenKrusty101

    GreenKrusty101 Initiate (0) Dec 4, 2008 Nevada

  18. TheHumanTorch

    TheHumanTorch Devotee (353) Jul 19, 2013 Connecticut

    So... Just looked back at the presentation. Allagash was seeing a 1 degree plato change in 3 weeks of conditioning. I remember the presenter saying that they had samples that they were still testing and the refermentation was still occurring. The batch in question was about a year old at that point

    Oregon State saw a 1 degree plato drop in dry hopped/reyeasted Coors-banquet vs. a control reyeasted coors. This was over 3 weeks.

    It seems as though the temp of these beers never went below 65F, although never fully clarified.

    OSU measured amyloglucosidase, alpha amylase, and beta amylase. Found traces of all 3 in cascade hops. Amyloglucosidase is used in the production of Brut IPA


    Edit: My personal experience is that you won't experience the same rate of change with beer in the 30-40F range.
     
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  19. GreenKrusty101

    GreenKrusty101 Initiate (0) Dec 4, 2008 Nevada

    Yes, I know, I've got one in the fermenter right now...@ 5 days it was @ 1.010...Co-pitched Imperial's Flagship and 5 ml of Glucoamylase...I'm going to go pull my 12 day sample right now...any guesses as to the gravity now? It's been at 65*F and started as a 1.059 OG Denali SMASH.
     
  20. GreenKrusty101

    GreenKrusty101 Initiate (0) Dec 4, 2008 Nevada

    Yes, I would like to guess that it is now 1.000 :grin: with amazing pseudo body for something that light.(I just sampled it)...it was incredibly bitter 7 days ago (probably a truby sample), but smooth as a baby's butt now...I'm stoked!
     
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