Cold crashing with a CCG

Discussion in 'Homebrewing' started by riptorn, Feb 28, 2021.

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  1. The_Modern_Brewhouse

    The_Modern_Brewhouse Initiate (195) Sep 25, 2020 Minnesota

    Hence my post #25.
     
  2. PortLargo

    PortLargo Pooh-Bah (1,831) Oct 19, 2012 Florida
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    I don't think I was taking a shot at your profit margin. I did question the reliability of low cost plastic parts. And throughout the thread I endorsed the concept of the product.

    I've been using your camlocks for years. Some time ago, in response to complaints about stiff cam arms (not from me), you explained that it was cost prohibitive to mill stainless for surgical grade smoothness. That makes sense . . . the product is practically indestructible, so what if there is some stiffness if the price reflects that. But I find lower-grade plastic parts in the brewhaus can be a problem. So when plastic is used, I have bought my replacements in advance. I also posted that the OP's results will override my doubt . . . so if the product is still working as designed in 4 years then the crow may be placed on my plate.

    Now that you're here, why don't you grab an Avatar and join some discussions? You might find the Home Bar Forum even more to your liking as it's more equipment focused. BTW, you have the most immaculate interior of a ferm fridge I've ever seen.
     
  3. riptorn

    riptorn Pooh-Bah (1,776) Apr 26, 2018 Georgia
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  4. VikeMan

    VikeMan Grand Pooh-Bah (3,067) Jul 12, 2009 Pennsylvania
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    @BrewHardware would be a welcome addition. He (Bobby) knows stuff.
     
  5. riptorn

    riptorn Pooh-Bah (1,776) Apr 26, 2018 Georgia
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    Post-Crash Temperature....would that be at the end of the cold crash (bottomed out), or packaging temp, which will be considerably higher?
     
  6. VikeMan

    VikeMan Grand Pooh-Bah (3,067) Jul 12, 2009 Pennsylvania
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    If they'll be different, then it's the temp at packaging. Since this whole thing will be sealed, the total CO2 pre- and post-crash will be the same. (And that total CO2 amount will be determined by all the pre-crash numbers, at a spunded equilibrium.) The final temperature, along with beer/fermenter headspace/bag volumes will tell us how it is (re)distributed.

    ETA: And if you're going to warm it up, try to estimate the bag volume right before packaging.
     
    #46 VikeMan, Mar 7, 2021
    Last edited: Mar 7, 2021
  7. riptorn

    riptorn Pooh-Bah (1,776) Apr 26, 2018 Georgia
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    They will be different. The beer will be raised to bottling temp of 68°, +/- 3°.

    The pre-crash bag volume is likely a bit less (probably < than a pint less) than 2.5 gallons due to the swapping out of the airlock to the CCG. Eyeballing it in its crashed environment, the bag volume has reduced no more than a quart, if that much.
    After the temperature rises it seems reasonable to expect the system pressure to be ~0.5psi (if the PRV is good), and the post-crash bag volume should be 2.5-gallons. Will post my observations.

    So far I've enjoyed this exercise, in part because the weather (highs in the mid 40's and lows in the upper 20's) has been conducive to crashing outside, au naturel.

    And here's the Outdoor Man cold crash bin:

    [​IMG]
     
    #47 riptorn, Mar 7, 2021
    Last edited: Mar 7, 2021
  8. VikeMan

    VikeMan Grand Pooh-Bah (3,067) Jul 12, 2009 Pennsylvania
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    So...this is the batch that was mostly airlocked and only "bagged" at almost the end? If so, I'm not sure we can make any good calculations about how much total CO2 you started with. If the bag had been attached and spunding for quite a while, we could assume 0.5 PSI, in equilibrium with the beer. But adding late, even if the bag (quickly) got to 0.5 PSI, the beer might not have had CO2 that reached a level that was in equilibrium. I guess we could assume it had reached equilibrium and treat it as an upper bound on how much CO2 was present, but realize that it was likely something less.
     
  9. riptorn

    riptorn Pooh-Bah (1,776) Apr 26, 2018 Georgia
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    Correct. It was ‘bagged’ almost at the end with a bag full of CO2 from a tank, via a swift as possible switchover from airlock/blowoff tube to the CCG. That probably resulted in a negligible, yet unknown, loss of CO2.

    Agree. An equilibrium @ 0.5 psi with the beer cannot be assumed at the start, or during the crash.

    The beer will be allowed to free rise to bottling temp over some days. I’ve attached tubing to the downstream side of the check valve, with the tag end of the tube in a jar of Starsan. As CO2 comes out of solution, and if the bag gets taught and there’s visible discharge into the jar, that will indicate the pressure has overcome the check valve and the system will be at 0.5 psi.

    The problem as I see it, and correct me if I’m wrong, is that equilibrium will be reached but there won’t be anything to assure it is at (or remains at) 0.5 psi without introducing CO2 under pressure. Maybe that’s just rephrasing what you said.

    A lot of variables, ifs, and unknowns in this trek. Some might think this is much ado about little, but it's definitely adding to my knowledge base.
     
  10. VikeMan

    VikeMan Grand Pooh-Bah (3,067) Jul 12, 2009 Pennsylvania
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    If the relief valve is operating properly, you shouldn't see any bubbling when it comes back up to temp, unless you bring it up to a temperature higher than the original fermentation temperature.
     
  11. PortLargo

    PortLargo Pooh-Bah (1,831) Oct 19, 2012 Florida
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    I would be in that camp. A couple of things: There is no real need to raise the temp for bottling. Not necessarily a problem but not a required step. I regularly cold crash in keg and transfer to bottling bucket at keg temp, add the sugar, and bottle. Yes, the beer temp is gradually raising during bottling and a smidgen of CO2 escapes. In theory the last bottle has less carbonation than the first . . . but this is the much ado part.

    You're fiddling around with 0.5psi pressures when the gauges we use don't accurately measure that precisely. Assuming you're using the standard homebrew-quality gauges (~10 bucks retail) that's just asking too much. I've compared my Taprite gauges to each other and it's common to be off 1psi . . . that's almost 10% in the range we're talking about. But when beer is force-carbonated there is no detectable difference in carbonation between the "high" gauge and "low" gauge. I have little faith those 0.5psi relief valves are really precision instruments. Again . . . much ado.

    Cold crashing and preventing the addition of oxygen is a wonderful thing and it sounds like your process worked. But I fall back to BF's advice of "use your judgement" . . . which is almost always the highest temp the beer was stabilized where CO2 could escape, typically the end of a diacetyl rest.
     
  12. riptorn

    riptorn Pooh-Bah (1,776) Apr 26, 2018 Georgia
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    I don’t have a bona fide, ideal temperature-controlled fermentation chamber. My stuff is a hybrid of Fred Sanford and Rube Goldberg.
    This was crashed outside with ambient temps from the mid-20’s to the mid-40’s. I put a heating mat around the ferm bucket (Inkbird controlled) as an attempt to keep it from getting too cold, and the bucket was placed in an outdoor storage box to help keep raccoons at bay. The beer temp did what I hoped it would do; dropped to ~39° over about 2 days and stayed within 2° of that until I brought it back inside.
    I had to leave the brewhouse for 7 days, starting yesterday. Before leaving, it seemed like a good idea to bring the bucket back inside to a more stable environment, rather than subject it to unknown changes in the weather over the next 6 - 7 days. Also before leaving, the bucket temp had risen to ~65° with no visually detectable increase in bag volume.
    Good to know that raising the temp is not necessarily a problem.

    We'll see. The jury is still out on whether it was an overall success. Hopefully I'll have a better idea of that in a few weeks.
     
    #52 riptorn, Mar 9, 2021
    Last edited: Mar 9, 2021
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  13. VikeMan

    VikeMan Grand Pooh-Bah (3,067) Jul 12, 2009 Pennsylvania
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    The bag should get bigger when the beer warms up. If it doesn't, that would suggest a leak somewhere.
     
  14. riptorn

    riptorn Pooh-Bah (1,776) Apr 26, 2018 Georgia
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    Yeah, that's what I thought as well.
    When making the switchover from the airlock to the CCG elbow fitting (through the airlock grommet), I thought, "hmmm, doesn't feel as snug as I thought it would." If that's the case, it would be like using a dry airlock and it avoided getting Srarsan in the beer, but not oxygen and potentially other undesirables :slight_frown:
     
  15. riptorn

    riptorn Pooh-Bah (1,776) Apr 26, 2018 Georgia
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    Before leaving for 6 full days, I put an Inkbird controlled (70°) heating mat around the ferm bucket. Inkbird was set at 70° with the heating differential set at 1°. Ambient temp never got above 66° while I was gone, so the cooling differential (also set at 1°) didn't come into play.
    I’m confident the beer temp didn’t go above 71° or below 69°, +/- a couple tenths?

    Got back today and the bag is taught, unlike what I saw at 65° the day before I left. I sprayed some Starsan around the airlock grommet (where the CCG elbow is inserted) and gave the bag a gentle squeeze....bubbles between the fitting and the grommet. So, that connection is not tight fit. If I use this again it will be after I get a fitting that fits more snugly in my airlock grommet.

    Planning to bottle this tomorrow.
     
  16. riptorn

    riptorn Pooh-Bah (1,776) Apr 26, 2018 Georgia
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    @VikeMan if it matters at this late stage, these are the values as close as I could determine. With the pre-crash bag volume and settled psi only eyeballed, this might be an exercise in futility. Maybe wait until/if I try the CCG again.....

    69° --------- Pre-Crash Temperature
    4.9-gal ---- Beer Volume
    2.9-gal ---- Fermenter Headspace Volume
    2.5-gal ---- Pre-Crash Inflated Bag Inner Volume (settled), less, but not a quart less
    0.5 psi ---- Pre-Crash Pressure (settled)
    _________

    70° -------- Post-Crash Temperature
     
  17. VikeMan

    VikeMan Grand Pooh-Bah (3,067) Jul 12, 2009 Pennsylvania
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    We can work with those numbers. One thing though... since the bag was inflated with CO2 from your tank, post-fermentation, and the fermenter had not been pressurized, you'd have a "regular" post-fermentation CO2 level (and pressure) in the beer and headspace at that point, and the bag would have been at 0.5 PSI (max, because of the valve). So the system could not have been settled at 0.5 PSI, as the beer had not been continuously pressurized at that level over time. But we can compute total system CO2, which is what matters.

    Beer CO2 @ 69F (20.6C) @ 1 atmosphere (0 PSI gauge) in 4.9 gallons (18.5 liters):
    = 18.5 * 1.977 * (0+14.695) * (0.01821 + 0.090115 * EXP(-1*20.6/23.95))
    = 30.3 grams

    Fermenter Headspace CO2 @ 20.6C @ 0 PSI gauge in 2.9 gallons (11 liters):
    = 11 * 1.977 * ((0+14.695) / 14.695) * (273.15 / (20.6 + 273.15)):
    = 20.2 grams

    Bag CO2 @ 20.6C @ 0.5 PSI gauge in 2.4 gallons (9.1 liters):
    = 9.1 * 1.977 * ((0.5+14.695) / 14.695) * (273.15 / (20.6 + 273.15)
    = 17.3 grams

    So, total system CO2:
    = 30.3 + 20.2 + 17.3 = 67.8 grams

    Since we know there are about 67.8 grams of CO2 in the system, we can use the above formulas to solve for the settled pressure and thus the beer CO2 volumes that result from 67.8 grams of CO2 at 70F, in 18.5 liters of beer, 11 liters of fermenter headspace and 2.5 gallons (9.5 liters) of bag headspace. It's an iterative process to solve, at least the way I did it, so I can't show it. But the answer is: 0.82 volumes of CO2, which is very close to what you'd expect at the end of a typical fermentation.

    I think this would be a much more interesting exercise with the guardian used during fermentation, so that a constant spunding pressure of 0.5 PSI would force additional CO2 to remain in the beer (and fermenter headspace). As it was, we just (more or less) computed a typical residual CO2 (plus a filled bag of CO2) and redistributed it slightly for equilibrium at a slightly different temperature. BTW, the formulas can be found in a few threads on another forum. I'm not posting them here out of respect for the Bros' turf.
     
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  18. riptorn

    riptorn Pooh-Bah (1,776) Apr 26, 2018 Georgia
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    For this Brown Ale, BrewCipher returned a quantity of 4.2 oz. corn sugar to achieve 2.3 vols. CO2. Not knowing when or if you’d get back with a detailed reply (apologies for doubting), I measured the priming sugar last night and reduced it to 3.9 oz for a projected 2.2 vols. CO2, just in case the system CO2 might be more than a regular, non-CCG’d fermentation.

    Based on your response, the difference in overall pre-packaged CO2 (regular v. CCG'd) is noise and I can weigh the corn sugar to suit me. Honestly tho', what’s +/- one-tenth volume of CO2 between friends?

    Disclaimer:
    Output can be no better than the inputs, and this run was rife with less-than-lab-quality measurements. Any lack of accuracy in predicting the outcome should not reflect on any of the contributors, except me.
     
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  19. PortLargo

    PortLargo Pooh-Bah (1,831) Oct 19, 2012 Florida
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    This was my hypothesis (and Brewer's Friend) from the beginning . . . 0,5psi can be ignored. While doing the math is interesting, it doesn't change much from "using your judgment". You have a good feel for where the temp was stabilized and CO2 was able to equalize. I've been doing this same drill for years with good results.

    For what's important: from your description, it appears the Guardian works as hoped for. The leaks you describe are manageable and it put to rest my doubts if the size was adequate. It's a shame BH didn't stick around for the victory lap. You probably aren't up for a true A/B test (who is?), but using the Guardian on an IPA might help prove it's attributes as the hop aromas age.
     
  20. riptorn

    riptorn Pooh-Bah (1,776) Apr 26, 2018 Georgia
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    Plus, for whatever solace it might be to me, the fermentor headspace (2.9 gallons) + the bag volume (2.5 gallons) exceeds the beer volume. Leaving the CCG attached will somewhat limit O2 during transfer, other than that which is in the bottling bucket pre-transfer (unavoidable in this scenario) and the CCG leak (avoidable in the future).
     
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