Filtering Beer Trouble

Discussion in 'Homebrewing' started by Aljossa, Jul 25, 2014.

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  1. ssam

    ssam Pundit (997) Dec 2, 2008 California

  2. koopa

    koopa Initiate (0) Apr 20, 2008 New Jersey

    Some people love gelatin and, if using a kettle fining to help coagulate protein like irish moss, it should work well. I myself have only used it twice and haven't been amazed by the results. But again, others have reported amazing results with it.

    I had a thought recently.....have all of your beers always been hazy or just your recent batches of kolsch? We seem to be focusing only on the idea that your most recent batches are hazy regardless of filtering (which is what makes me think chill haze is to blame). If they all have been hazy, what is your water like? If your water is very soft (less than 50 ppm of calcium to be specific) it can greatly inhibit your beers ability to clear.
     
  3. Aljossa

    Aljossa Initiate (0) Jul 25, 2014 Serbia

    Yes, all my beers, not just Kolsch, were always cloudy. And regarding hardness of water, I just can't give you an answer. I didn't check that. I'm using RO three stage filter to clear our tap watter from unwanted elements. But I had one batch using water from my well, and the results were just the same. And how can you explain that beer is clearing after long time, if the blame is on hardness of water? Because that variable is constant, despite the time.
     
  4. VikeMan

    VikeMan Grand Pooh-Bah (3,067) Jul 12, 2009 Pennsylvania
    Pooh-Bah

    I may have missed something along the way, and if so, sorry. But it sounds like you are mashing with Reverse Osmosis water (i.e. water with very little minerals...close to zero if your RO filter is efficient). If so, and if you're not adding minerals back in, you are missing Calcium, which is important to yeast flocculation. That could very easily explain cloudy beer that clears much later.
     
  5. Tebuken

    Tebuken Initiate (0) Jun 6, 2009 Argentina

    So, how“s your mash efficiency?, if you use just RO water to mash without adding acid malt to low mash Ph(pale beers) or baking soda to raise mash Ph(dark beers),calcium chloride and/or calcium sulfate I don“t think you get the proper mash Ph for brewing every beer style , neither enough calcium to get a good fermentation.
     
  6. Aljossa

    Aljossa Initiate (0) Jul 25, 2014 Serbia

    Have to say that I didn't know that! Tnx for the tip, I'll for sure check pH of my next brew. When I should measure it? After I add malt into 45 degrees Centigrade water?
     
  7. Aljossa

    Aljossa Initiate (0) Jul 25, 2014 Serbia

    Bcs of your post I've just started reading about pH of the mash and find out a lot about it. Tnx for hint, since I didn't check that element at all!? So, if I'm brewing Kolsch, then my target pH should be 5.2, if I understood right?
     
  8. VikeMan

    VikeMan Grand Pooh-Bah (3,067) Jul 12, 2009 Pennsylvania
    Pooh-Bah

    My tip (the one you quoted) was not about pH. It was about having enough calcium for yeast flocculation. But calcium also affects mash pH, which is important too (though not necessarily associated with yeast flocculation as far as I know).
     
  9. jbakajust1

    jbakajust1 Pooh-Bah (2,552) Aug 25, 2009 Oregon
    Pooh-Bah

    Target pH is always 5.2. But you will want different levels of Calcium, Magnesium, Sodium, Sulfate, Chloride, and Carbonate to give you the correct flavor profile for each style you are brewing.
     
  10. Aljossa

    Aljossa Initiate (0) Jul 25, 2014 Serbia

    I was actually reading on the internet that pH of the mash is directly related to the Calcium concentration. Am I wrong? Is that meaning that I should control two variables now? Both pH and minerals concentration in the mash?
     
  11. Aljossa

    Aljossa Initiate (0) Jul 25, 2014 Serbia

    OK, but for Calcium levels are different for different styles of beers? I've just read somewhere that it is the best to have Ca levels from 50 - 150 ppm for pale beers?
     
  12. VikeMan

    VikeMan Grand Pooh-Bah (3,067) Jul 12, 2009 Pennsylvania
    Pooh-Bah

    Adding calcium to the mash is one way to lower mash pH. You can also lower the mash pH by using more (or different) specialty malts, or by adding an acid (such as phosophoric acid or lactic acid).

    But as far as calcium aiding in yeast flocculation...the calcium doesn't necessarily have to be in the mash. It can be added in the kettle.
     
  13. Aljossa

    Aljossa Initiate (0) Jul 25, 2014 Serbia

    S
    So, what actual procedure should be? What should I check, pH or hardness of mash? If ph is bellow 5.2 then too add bicarbonate and if it is over 5.2 to ad some salt with Calcium, or to use acid malts (1% for 0.1 pH)?
     
  14. Aljossa

    Aljossa Initiate (0) Jul 25, 2014 Serbia

    Question is the same then? What should I be checking? pH or hardness of mash in order to achieve target of 5.2?
     
  15. VikeMan

    VikeMan Grand Pooh-Bah (3,067) Jul 12, 2009 Pennsylvania
    Pooh-Bah

    You don't need to check the hardness of the mash. But if you know your starting water profile, you can compute the various ion levels that will result from adding whatever brewing salts (like Gypsum or Calcium Chloride, etc.) you plan to add.

    I would recommend starting by reading this link...
    https://sites.google.com/site/brunwater/water-knowledge
    And/or read the white papers on mash pH at...
    http://homebrewingphysics.blogspot.com/
    The latter are a little more technical than the former, but very informative.

    Once you have some basic knowledge, there are several competent mash pH tools available...
    Bru'nWater
    EZWater
    MpH Calculator
    BrewCipher (which is also a general brewing spreadsheet, so the water calcs are automatically integrated with your recipe. I recommend BrewCipher because it's mine, and because it has the excellent MpH calculator models embedded in it)
     
  16. Tebuken

    Tebuken Initiate (0) Jun 6, 2009 Argentina

  17. koopa

    koopa Initiate (0) Apr 20, 2008 New Jersey

    Also note that if you do a pH measurement of a mash sample, you should let it cool down first before taking it. If you take it at mash temperature, it could potentially be 0.35 higher. In other words, a target mash pH of 5.2 is the measurement of a cooled sample. The same sample at mash temperature will be roughly 5.5 - 5.6 pH. It is also not the best for the life of the pH pen's measurement probe to take mash temperature readings.
     
  18. Aljossa

    Aljossa Initiate (0) Jul 25, 2014 Serbia

    Joint question for koopa, Tebuken, VikeMan...

    By what I've read on the links mentioned above + what your suggestions are regarding water, here are some of the questions, conclusions, ideas I have:
    Since I'm using three stage RO filter it looks like that I'm striping my (tap) water from not just chlorine, but also all minerals. Most important of all of them is Calcium. So, if I would like to use that water for brewing, then I should temper it by adding compounds like CaCl2, CaCO3. Then my pH will be changed in accordance with adding of some of those salts. CaCl2 will make my water (or mash) more acid (pH under 7) while adding CaCO3 will make it more alkaline. So then, I'll need to add acids, if the pH is above 5.2-5.8 range or to use acid malts. Or if the environment is very acid (bellow 5.2) I'll need to add NaHCO3 in order to make it more alkaline. That will further change levels of Potassium, Carbonates, etc. in my water/mash. So many variables and so easy to get it wrong.

    Instead of all of that, how about following?
    Ditching three stage RO filter and just keep active charcoal filter which will remove Chlorine from water and in the same time keep all necessary minerals (Ca, Mg, Na) for particularly fermenting.
    Then checking pH and if it is to high (what is most likely, since most of the tap waters are more alkaline than acidic), to use acid malts in order to lower pH during mashing/boiling.
    My concern here is that using those malts could change my original beer recipe and hence change beer taste accordingly. That's something I would also like to avoid. Adding some acids is also option hard to swallow. Maybe drop or two of H2SO4 could be acceptable, I think.

    Adding chemical compounds like CaCl2 is something I would like to avoid, since number of them are labeled as "taste enhancers" and have infamous E labels. I think that CaCl2 is E-509 and having this on the label of my beer, would be such a turn off for consumers and also it will be so hard for me to sell my beer, saying that it is made from only four ingredients: water, malt, hops and yeast.

    Am I on a right track, please?
     
  19. VikeMan

    VikeMan Grand Pooh-Bah (3,067) Jul 12, 2009 Pennsylvania
    Pooh-Bah

    There are many variables. But it's not difficult to get it right. As long as you know what your starting water profile is, and what your goals are, the spreadsheets do the math for you as you build.

    Mg and Na aren't really needed for fermenting. Ca does help yeast flocculation. You can certainly use your carbon filtered tap water, but it won't be ideal for every style. Maybe not even ideal for one style. But yes, if you have reasonably hard water, you have enough Ca to get cover what the yeast will need.

    You can check mash pH and see what kind of pH adjustment is needed. But it's also helpful to be able to predict what that pH will likely be, plan the major adjustments accordingly, and start your mash with those adjustments. Then if further a adjustment is needed (after measuring actual mash pH), it will be a small adjustment.

    Acid malt is just pilsner malt with lactic acid. The amount of acid malt you might typically need to use won't change the original recipe significantly. I would not recommend Sulfuric Acid (H2SO4). Lactic or Phosphoric would be a better choice.

    Okay, so if it's important to not use any 'chemical compounds' and you want to make beer good enough that people will want to buy it... my recommendation would be to get an analysis of your carbon filtered water and then figure out what styles of beer might match up well with your water. i.e. if you don't want to change your water, brew to your water's strengths.
     
  20. Aljossa

    Aljossa Initiate (0) Jul 25, 2014 Serbia

    Tnx for thoughts.

    Why would you suggest to avoid H2SO4? Btw, I've just read somewhere that acid is being used for pH adjustments of vine before fermentation starts. They need to lower their pH to something as low as 3.3
     
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