Low Oxygen Brewing

Discussion in 'Homebrewing' started by OldBrewer, Apr 10, 2018.

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  1. OldBrewer

    OldBrewer Maven (1,385) Jan 13, 2016 Canada (ON)

    Yes, it was in response to your post. I'm confused - you said that you remove the water from the mash tun (plastic cooler), leaving a thhick wort behind, and then "boil the wort". Since the thick wort is still in the cooler, how do you boil it?
     
  2. OldBrewer

    OldBrewer Maven (1,385) Jan 13, 2016 Canada (ON)

    The only way that sort of makes sense is if you're only boiling the thin wort that has been drawn off from the thicker wort in the mash tun - which is a backward apporach. If so, I'm not really sure that you can call it "decoction brewing". My understanding is that you always boil the thicker portion - the one with the most grain. The melanoidins come from the grain, not the water. Your approach sounds more like a step mash approach.
     
  3. VikeMan

    VikeMan Grand Pooh-Bah (3,067) Jul 12, 2009 Pennsylvania
    Pooh-Bah

    It's called a thin decoction. It's a thing. And it is a type of step mash, as is a thick decoction.
     
  4. invertalon

    invertalon Pooh-Bah (2,249) Jan 27, 2009 Ohio
    Pooh-Bah Trader

    Yes, more of this approach vs a thick decoction. Not exactly same, I know... For some reason I misread the post and thought a thinner decoction was desired. My bad!
     
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  5. OldBrewer

    OldBrewer Maven (1,385) Jan 13, 2016 Canada (ON)

    No problem. At least now I understand why I was confused by your reply.
     
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  6. OldBrewer

    OldBrewer Maven (1,385) Jan 13, 2016 Canada (ON)

    Yes, both can be considered as part of a step mash. I guess where strict definition is considered, a "decoction" does not have to involve the thicker portion. I'm not sure what the correct definition is when you boil the thicker portion. Maybe it needs a new term to help avoid confusion.
     
  7. Brewday

    Brewday Zealot (721) Dec 25, 2015 New York

    I think they use the pump for convenience and keeping the wort hot.I would assume if your boiling the decoction your're deaerating so pouring it back hot should be ok. If this was a problem then lautering would be a issue.
     
  8. OldBrewer

    OldBrewer Maven (1,385) Jan 13, 2016 Canada (ON)

    Yes, the boiled decoction will have been de-aerated, but if the boiled decoction is dumped into the rest of the mash, that would aerate the resultant mash. I guess one could ladle it in carefully, but doing so will greatly decrease the resultant temperature (the initial range of temperature of boiled wort drops rapidly with time), resulting in a difficult to estimate combined mashing temperature.
     
  9. hopfenunmaltz

    hopfenunmaltz Pooh-Bah (2,635) Jun 8, 2005 Michigan
    Pooh-Bah

    Boiling the thin part is usually the last step. You are denaturing the enzymes if you do this. The fist steps boil the thick part which explodes starch making it more available to the enzymes once the non boiled liquid is introduced. Maillard reactions also occur.

    The next time I'm in a big brewery I might ask to see the mash transfer pumps that move the mash from the mash tun to the lauter tun.
     
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  10. gold_strong-ales_worldcup

    gold_strong-ales_worldcup Initiate (0) Dec 2, 2018

    As a pro, I add O2 inline to the fermenter as that's how the brewery is plumbed. In that case, O2 necessarily comes before pitching. At home, I pitch a half cup of low generation yeast into the carboy first. When full, I use a .5 micron stone at the lowest pressure, put it in the center of the carboy and don't move it for five minutes until shut-off. According to my scale, weighing my 02 tank afterwards, I'm using 3.5 grams O2 in 5 minutes at trickle feed and am yielding optimal efficiency and results. Oddly, the tank says 40 grams on the label, but the scale always shows 70 grams in a full tank, not just 40. That's 20 batches or 50 cents per batch per $10 bottle, which seems a small price to pay for oxygenation at such a high degree of purity, especially for those who like to repitch multiple times. I'll go pure 02 over mixing-in airborne contaminants every time.
     
  11. OldBrewer

    OldBrewer Maven (1,385) Jan 13, 2016 Canada (ON)

    O2 is indeed important during the immediate time of fermentation. However, the key to low oxygen brewing is to prevent as much oxygen as possible from entering the mash/wort during any part of the process prior to fermentation.
     
  12. pweis909

    pweis909 Grand Pooh-Bah (3,250) Aug 13, 2005 Wisconsin
    Pooh-Bah

    @gold_strong-ales_worldcup
    Great idea to weigh the O2 tank. I’ve always thought of oxygenation as pretty inexact but this approach to put some numbers on it had always been in reach. Just never occurred to me.
     
  13. hopfenunmaltz

    hopfenunmaltz Pooh-Bah (2,635) Jun 8, 2005 Michigan
    Pooh-Bah

    Sierra Nevada uses sterile filtered air for their ales. Sometimes I use an aquarium pump with an inline hepa filter.
     
  14. riptorn

    riptorn Pooh-Bah (1,776) Apr 26, 2018 Georgia
    BA4LYFE Society Pooh-Bah Trader

    Same here.
    According to several online sources, air by volume is ~78% nitrogen, ~21% oxygen, ~ 1% argon and considerably lesser amounts of CO2 and other gasses.
    I wonder how the makeup of air affects our "oxygenation", and whether suggestions to aerate as we do via a pump and stone method for XX seconds accounts for air being only 21% oxygen?
     
  15. billandsuz

    billandsuz Pooh-Bah (2,097) Sep 1, 2004 New York
    Pooh-Bah

    Using an air pump and a stone will get you up to about 8 ppm Oxygen in room temp wort and no more. And it will hold the oxygen pretty well too.

    Using a bottle of pure Oxygen and a stone allows for much more saturation, up to 20 ppm or more of Oxygen in solution. I have seen the meter get above that number too though it's just wasting expensive bottled gas.

    The thing is however, even if you can saturate the wort to 20 ppm, it doesn't mean it's better. How much oxygen is enough and how much is too much is another discussion.
    Importantly the dissolved Oxygen falls off pretty rapidly anyway, and will settle down to around 12 ppm when using a bottle.

    Cheers.
     
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  16. epk

    epk Pundit (849) Jun 10, 2008 New Jersey

    I always wondered this myself. At room temp, isn't the O2 coming out of solution rather quickly? I also wonder about headspace. Can yeast utlize O2 simply in the headspace? We always talk about yeast scrubbing O2 from bottles - obviously that's a much smaller area - but would that work the same way for fermentor headspace?
     
  17. minderbender

    minderbender Initiate (0) Jan 18, 2009 New York

    The solubility of oxygen in the wort is a function of the partial pressure of oxygen in the head space. So the more oxygen is in there (vs. other gases), the less oxygen should come out of solution. To put it another way, an equilibrium should form that balances the oxygen leaving the wort into the headspace and the oxygen going in the other direction. As the yeast consume oxygen, they should disrupt that equilibrium and draw more oxygen down into the wort. However, once the yeast start producing significant amounts of carbon dioxide, the partial pressure of oxygen in the head space should fall dramatically as CO2 enters the headspace and a mix of oxygen and CO2 exits via the airlock.
     
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  18. epk

    epk Pundit (849) Jun 10, 2008 New Jersey

    There it is, that's the bit I was trying to visualize in my mind. I mostly get the science around pressure equilibrium and such after years of kegging and cold crashing, I was just missing that part in my mind. That the O2 in the headspace can actually be drawn into the wort. Make sense, thanks. I assumed some of it got utilized in some fashion.

    At the same time, it would also be reaching an equilibrium with pressure outside the fermentor (unless it was sealed), so O2 coming out of solution would also potentially seep right out the airlock even before fermentation starts going, no?
     
    #138 epk, Dec 3, 2018
    Last edited: Dec 3, 2018
  19. minderbender

    minderbender Initiate (0) Jan 18, 2009 New York

    Yes, but the rate of gas exchange is also a function of the surface area, and the surface area of the liquid in the airlock is miniscule, especially compared to the large interface between the wort and the headspace. I think of it kind of like "the dose makes the poison"—if a rate is slow enough, you can basically treat it as zero. Hawaii is inexorably sinking beneath the waves (perhaps to be replaced by new volcanic islands, which in turn will meet their fate), but it is happening on a timescale that can be safely ignored for vacation planning purposes.

    [Edited to add... I kind of went off on a tangent about long-term aging. For the, like, 12-24 hours during which the yeast is growing but not producing much CO2, you would lose a negligible amount of oxygen through gas exchange in the airlock. Same concept as what I described, but I focused on longer-term concerns.]

    So yeah, very slowly the gas in the headspace should approach the balance of gases in the atmosphere (the airlock fluid should be absorbing CO2 from the headspace and releasing it into the atmosphere, and absorbing O2 from the atmosphere and releasing it into the headspace). But I can't emphasize enough how slow this process is. This summer I aged a sour beer for about 8 months in a Fermonster plastic fermenter with about 1.5 gallons of headspace, under a vodka-filled airlock (which I kept topped up pretty assiduously). I recently started drinking the beer, and I think there's a hint of acetic character, indicating some oxygen exposure. (This was not undesired.) But I'm quite certain that if I left a glass out overnight, the beer would change a lot from the new oxygen exposure. In other words, even after 8 months of equlibrating toward atmospheric conditions, the headspace was still very protective of the beer. (There was also a pellicle, but I doubt it was very important. Maybe more importantly, there was definitely Brettanomyces in the beer, which may have helped scavenge oxygen. Still, the point mostly stands.)

    So for a clean beer, where it might sit under the airlock for 2-4 weeks, the oxygen ingress is pretty minimal.

    [Edited for emphasis.]
     
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  20. billandsuz

    billandsuz Pooh-Bah (2,097) Sep 1, 2004 New York
    Pooh-Bah

    An easy way to visualize pressure equalization of gas in liquid and atmosphere is to consider an open bottle of beer or soda.

    CO2 molecules will leave the liquid until the pressure in atmosphere is equilibrated. That is, the beer will go flat, because the dissolved CO2 that we forced into the liquid is much greater than the gas pressure in atmosphere. And conversely, Oxygen will be absorbed until the pressure in atmosphere is equal to the amount of Oxygen in the liquid.

    I use this explanation many times describingto clients how a CO2 regulator works to keep a keg carbonated. It's not really a hard concept if it is visualized.
     
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