Measuring LME

Discussion in 'Homebrewing' started by CarolusP, Feb 17, 2016.

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  1. CarolusP

    CarolusP Zealot (590) Oct 22, 2015 Minnesota

    I put together a quick batch of extract beer last week. The recipe that I created used 6lbs of LME and 1lb of DME. Running the recipe through Brewers Friend, I should have had an OG of 1.046 with a volume of 5.5gal, but I ended up with an OG of 1.052. I corrected my gravity reading for temperature, and I've validated with plain water that my hydrometer is calibrated correctly. I'm quite certain that I didn't misread my gravity reading.

    Short of a neighbor kid sneaking into my garage and throwing a bag of jelly beans into my boil when I wasn't looking, I'm a little floored as to where my extra gravity came from. I wondered if when LME is sold in 6 lb cartons, are they actually giving you about 6.5 lbs with the expectation that due to the viscosity of the syrup, that a fair amount of the extract will be left in the carton. Has anyone ever actually weighed out a carton of LME to see if this is the case? When I use LME, I put hot tap water into the carton after the initial pour, give it a good shake and add it to the boil; so I basically get every drop out of the carton. Granted that if this was the difference, it would only make about a 3-4 point difference in my overall gravity, but that would at least account for most of the discrepancy.
     
  2. OldBrewer

    OldBrewer Maven (1,385) Jan 13, 2016 Canada (ON)

    My calculation shows a result of 1.048, which is still a little short. Did you add any specialty malts? They do add a few points.

    LME: (36.8 x 6)/5.5 = 40.15
    DME: (45.0 x 1)/5.5 = 8.18
    40.15 + 8.18 = 48.33 Therefore 1.048

    Plus specialty grains (1 - 2 pounds could easily give you the missing gravity).
     
    #2 OldBrewer, Feb 17, 2016
    Last edited: Feb 17, 2016
  3. ssam

    ssam Pundit (997) Dec 2, 2008 California

    My best guess is you ended up with less volume than you expected.

    I've seen my LHBS fill LME and they stop at 6lbs. That hot water thing is pretty much standard practice and I'm sure other LME people know you'll do that.

    Oh, also DME adds more gravity per unit weight, did you account for that in your calcs?
     
  4. OldBrewer

    OldBrewer Maven (1,385) Jan 13, 2016 Canada (ON)

    I should mention that there is a range of potential gravities for both LME and DME depending on the manufacturer:

    LME: 1.034 - 1.038
    DME: 1.040 - 1.045

    Thus, depending on the extracts you used, the specific gravity of the wort (assuming using only 6 pounds of LME and 1 pound of DME), could range from 1.044 - 1.050. Different calculators use different assumptions regarding the potential gravities of the two extracts. The better ones should either provide a range, or allow you to enter (or change) the assumed potential gravities of the two extracts.
     
    #4 OldBrewer, Feb 17, 2016
    Last edited: Feb 17, 2016
  5. CarolusP

    CarolusP Zealot (590) Oct 22, 2015 Minnesota

    @OldBrewer - No, I didn't add any specialty malts or grains. This was all extract.

    @ssam - I sent 5.5 gallons into the fermenter. The LME was Maillard Malts, which has 36ppg. The DME was Breiss, which is 43ppg.

    I ran everything through Brewers Friend, but doing the math manually:

    LME: 36*6 = 216
    DME: 43*1 = 43

    216+43 = 259
    259/5.5 = 47
     
  6. JackHorzempa

    JackHorzempa Grand Pooh-Bah (3,375) Dec 15, 2005 Pennsylvania
    Society Pooh-Bah

    How exactly did you measure the wort volume. Was trub a part of this volume?

    Cheers!
     
  7. CarolusP

    CarolusP Zealot (590) Oct 22, 2015 Minnesota

    I have markings on my stirring stick that I use to measure while in the kettle. My carboy also has lines on it confirming the 5.5 gallons.
     
  8. pweis909

    pweis909 Grand Pooh-Bah (3,250) Aug 13, 2005 Wisconsin
    Pooh-Bah

    3-4 points seems like it could be a combination of hydrometer error, measurement error, mixing/dilution error, volume error, batch to batch variation in LME concentration, and minor ruptures in the space time continuum. Nothing to sweat over. If you are convinced it is none of these possibilities, perhaps you suffer from overconfidence.
     
  9. OldBrewer

    OldBrewer Maven (1,385) Jan 13, 2016 Canada (ON)

    Actually, it's more like 5 points, which is fairly significant. Not only that, I find the difference intriguing, since, in addition to brewing, I for one, am fascinated with the math behind brewing, and have written - and use - all my own formulas for all aspects of brewing. I do have BeerSmith but rarely use it since the math itself is so much fun for me, and using the formulas allows me to have a better insight in what's actually happening while brewing. It's a bit like being excited about detective work.

    So even while I agree that there's little to worry about in terms of the final product, it's still educational for some to try to figure out why there's such a difference. Knowing these things helps all of us improve our understanding of the brewing process and allow us to keep improving our beers. Otherwise we would still be making the same crappy beers from 1.5 Kg. Muntona and other can kits that were common during the early nineties.
     
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  10. JackHorzempa

    JackHorzempa Grand Pooh-Bah (3,375) Dec 15, 2005 Pennsylvania
    Society Pooh-Bah

    And the answer to: "Was trub a part of this volume?"

    Cheers!
     
  11. JackHorzempa

    JackHorzempa Grand Pooh-Bah (3,375) Dec 15, 2005 Pennsylvania
    Society Pooh-Bah

    That is a fair bit of hyperbole. Being 'off' on the OG by a few points (whether it be 5 points or 3-4 points) is nothing like what you are stating here.

    Cheers!
     
  12. OldBrewer

    OldBrewer Maven (1,385) Jan 13, 2016 Canada (ON)

    No, there's certainly a huge gap. But I was referring to all the minor and major improvements over the years leading to the excellent homebrewing knowledge, equipment and ingredients we have today. Every little bit along the way has led to this.
     
  13. CarolusP

    CarolusP Zealot (590) Oct 22, 2015 Minnesota

    I'm not sure what you mean by the question. I did a 5.5 gallon volume so that I would still have about 5 gallons of beer once removed from the trub.
     
  14. CarolusP

    CarolusP Zealot (590) Oct 22, 2015 Minnesota

    It's certainly not above me to commit error. My first child was born a few days before doing this batch, so being as low on sleep as I was, I was making extra sure to measure as carefully as possible. If it were a mere few points off, I would have written it off as nothing. Five points seemed a bit odd. I know the beer will still turn out fine...I posed the question more out of curiosity than anything else.
     
  15. pweis909

    pweis909 Grand Pooh-Bah (3,250) Aug 13, 2005 Wisconsin
    Pooh-Bah

    I can easily shrug my shoulders at your 5 points. Our measurement devices are imperfect, and people make mistakes in measurement, and your calculations do not appear to account for these things. Sorry, @CarolusP, but your assertion that you were being extra careful despite being low on sleep would not hold up in court. "Yes, your honor, I had been drinking, but that is precisely why I was being extra careful!"
     
  16. OldBrewer

    OldBrewer Maven (1,385) Jan 13, 2016 Canada (ON)

    I'm with you, Carolus. it's easy to shrug off all errors, but only by looking more deeply into and studying errors do we progress in our knowledge and understanding of the process.

    A range for the error has already been established, yet the error is still 5 points outside of that range. If it had been within that range, the error could easily have been shrugged off. The calculation is simple and there are very few variables, unlike mashing. Thus, logically, there must be something else that we are yet missing. Most of the errors in measurement that could have caused this much variation have been reasonably ruled out, and it's hard to believe that the potential gravity of either the LME or DME would fall that far outside of the range commonly accounted for.

    So, the only variable that I can think of that has not yet been addressed is the temperature of the wort when you measured the volume. Water expands when heated, so if you measured the 5.5 gallon volume when hot, you would not have an accurate measure of the volume. It would actually be less than 5.5 gallons when cooled to room temperature, driving up the SG. Do you know what the temperature of the wort was when you measured the volume on your stir stick?
     
  17. ssam

    ssam Pundit (997) Dec 2, 2008 California

    Um, does it? I've never had my water expand before, unless I turned it into ice or vapor.
     
  18. OldBrewer

    OldBrewer Maven (1,385) Jan 13, 2016 Canada (ON)

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  19. CarolusP

    CarolusP Zealot (590) Oct 22, 2015 Minnesota

    It does expand. The factor I've read is 4% difference in volume between chilled wort vs. boiling wort, which in a 5 gallon batch would account for about 1/5th of a gallon difference. In a rolling boil, there would be additional volume increase due to the displacement caused by the bubbles rising from the bottom of the pot, but I'm not sure exactly how much displacement this causes.

    In my case, I accounted for it since 5.5 gallons of chilled wort is what went into the carboy.
     
  20. ssam

    ssam Pundit (997) Dec 2, 2008 California

    Right, I guess I never noticed because of the negligible change on the volumes I use. I suppose it could make a difference in a 5 gallon batch.
     
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